Logo UAB

Basic Experimentation in Chemical Engineering

Code: 106054 ECTS Credits: 6
2024/2025
Degree Type Year
2500897 Chemical Engineering OB 1

Contact

Name:
Xavier Font Segura
Email:
xavier.font@uab.cat

Teachers

José Luis Montesinos Seguí
Francisco Valero Barranco
Kírian Bonet Ragel
Eric Valdes Martin
Marina Guillen Montalban
Francisco Javier Guerrero Camacho

Teaching groups languages

You can view this information at the end of this document.


Prerequisites

Having studied the subject of Chemical Engineering Fundamentals. Understanding Catalan, since the lab-guides are written in Catalan.


Objectives and Contextualisation

The objectives of the course are:

  • Reach a minimum level of knowledge of basic concepts in the field of TIC that will include the writing of reports, bibliographic search and the use of MS Word, PowerPoint and Excel.
  • Experimental verification of different basic aspects of chemical engineering. These aspects include: the heat energy and matter balance and the experimental determination of the transport properties of diffusivity of a component and viscosity.

Competences

  • Apply scientific method to systems in which chemical, physical or biological transformations are produced both on a microscopic and macroscopic scale.
  • Assume the values of professional responsibility and ethics required in chemical engineering.
  • Communication
  • Demonstrate basic knowledge of the use and programming of computers, and apply the applicable IT resources to chemical engineering.
  • Develop personal attitude.
  • Develop personal work habits.
  • Develop thinking habits.
  • Observe ethics and professionalism.
  • Students must be capable of applying their knowledge to their work or vocation in a professional way and they should have building arguments and problem resolution skills within their area of study.
  • Students must be capable of collecting and interpreting relevant data (usually within their area of study) in order to make statements that reflect social, scientific or ethical relevant issues.
  • Students must have and understand knowledge of an area of study built on the basis of general secondary education, and while it relies on some advanced textbooks it also includes some aspects coming from the forefront of its field of study.
  • Understand and apply the basic principles on which chemical engineering is founded, and more precisely: balances of matter, energy and thermodynamic momentum, phase equilibrium and kinetic chemical equilibrium of the physical processes of matter, energy and momentum transfer, and kinetics of chemical reactions
  • Work in a team.

Learning Outcomes

  1. Apply matter and energy balances to continuous and discontinuous systems.
  2. Apply scientific method to perform macroscopic balances of matter, energy and momentum.
  3. Communicate efficiently, orally and in writing, knowledge, results and skills, both professionally and to non-expert audiences.
  4. Design experiments.
  5. Develop critical thinking and reasoning
  6. Develop independent learning strategies.
  7. Develop scientific thinking.
  8. Maintain a proactive and dynamic attitude with regard to one's own professional career, personal growth and continuing education. Have the will to overcome difficulties.
  9. Manage available time and resources. Work in an organised manner.
  10. Perform a critical analysis of experimental results and of the overall work done.
  11. Prevent and solve problems.
  12. Respect diversity in ideas, people and situations.
  13. Students must be capable of collecting and interpreting relevant data (usually within their area of study) in order to make statements that reflect social, scientific or ethical relevant issues.
  14. Students must have and understand knowledge of an area of study built on the basis of general secondary education, and while it relies on some advanced textbooks it also includes some aspects coming from the forefront of its field of study.
  15. Use spreadsheets and numerical programming environments to solve chemical engineering problems.
  16. Work autonomously.
  17. Work cooperatively.

Content

The contents of the subject are divided into two different parts, each corresponding to 3 ECTS: Basic Practices in Computer Science and Laboratory Practices in Bases in Chemical Engineering

Basic practices in computer science

  • Microsoft Word: Application to the writing of technical reports:
    • Formatting a technical document.
    • Automatic generation of Tables of contents.
    • Tools for bibliographic searches.
    • Bibliographic citations in documents.
  • Microsoft Excel Application to Engineering problems:
    • Work environment. Basic operation and formulas.
    • Functions preprogrammed to Excel.
    • Graphical representations and regressions.
    • Programming logic statements.
    • Vectors and matrices.
    • Integration and numerical derivation.
    • MS Excel tools and add-ins. The "Solver".

Laboratory practices of Bases in Chemical Engineering

They will take place within the last 7 weeks of the second semester. It consists of 5 practices that will be carried out in the laboratory.

  • Basic chemical laboratory techniques.
  • Heat energy balance.
  • Material balance of a component.
  • Determination of the diffusivity of a component.
  • Determination of viscosity.

Activities and Methodology

Title Hours ECTS Learning Outcomes
Type: Directed      
Presentación y funcionamiento de la asignatura 2 0.08 11
Type: Supervised      
Realización de las pràcticas 75 3 1, 5, 8, 9, 10, 12, 17
Type: Autonomous      
Elaboración de informes y resolución de problemas 69 2.76 1, 2, 3, 5, 7, 9, 10, 13, 14, 15

The methodology of the course is based on conducting the aforementioned practicals in the computer room or laboratory. The practicals on computer science fundamentals will be preceded by a brief theory session. To carry out the laboratory practicals, students will have a guide for each practical that they must read and prepare before the start of each practical session.

Since this is an eminently practical learning experience, attendance at the practical sessions (both computer and laboratory) is mandatory.

Depending on the number of students, the academic calendar, the capacity of the computer room, and the number of experimental installations, students will be divided into different shifts and groups of 2 students (if possible). For the computer science practicals, these will be conducted in the morning, while for the laboratory practicals, there will be both morning and afternoon shifts. The student groups do not have to be the same for the computer science practicals and the laboratory practicals.

A preliminary presentation session will be held at the start of the laboratory practicals.

Laboratory Practicals in Chemical Engineering

It is important to have the practicals prepared before entering the laboratory. Students will know in advance which practical they need to do on each occasion, and they will have the necessary information on the Virtual Campus, allowing them to come prepared. Each student must have a laboratory notebook of at least A5 size, in which they will prepare the practical before entering the laboratory on the day of each practical. If not, they will have to leave the laboratory to read and prepare the practical.

Prior to the start of the practicals, in a mandatory session for all students enrolled in the course, the operation of the laboratory, the practical schedule, and the use of the notebook will be explained.

General Safety Rules in the Laboratory

On the first day of practical work in the laboratory, not the course presentation day, students must submit to the professors the signed document generated upon passing the "Laboratory Safety" test. The test is available on the Virtual Campus. It is mandatory to wear a lab coat, have note-taking material, and have previously studied the guide of the practical to be performed, in addition to following the safety rules mentioned on the Virtual Campus.

Annotation: Within the schedule set by the centre or degree programme, 15 minutes of one class will be reserved for students to evaluate their lecturers and their courses or modules through questionnaires.


Assessment

Continous Assessment Activities

Title Weighting Hours ECTS Learning Outcomes
Actitud al laboratori 7.5% 0 0 3, 8, 11, 17
Informatics Exam 50% 2 0.08 6, 9, 15, 16
Informes Laboratorio 35% 0 0 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 12, 13, 14, 15, 16
Lab Exam 7.5% 2 0.08 13, 14

Process and Scheduled Assessment Activities

The evaluation of the two parts of the course is independent, and a minimum grade of 5 in each part is required to average them.

Computer Science Fundamentals Practicals

Assessment will be based on different exercises that must be submitted at the end of the session. To pass this part of the course, a grade of 5.0 out of 10 or higher is required on average across the various continuous assessment activities.

Chemical Engineering Fundamentals Laboratory Practicals

Attendance at all laboratory sessions is mandatory to pass the course. Additionally, the assessment activities include:

  • Presentation of reports for each practical: All reports must be submitted, and a minimum average of 5.0 out of 10 in the report grades is required to pass the course. The schedule for report submission will be notified before the start of the laboratory practicals. Late submission will result in a penalty on the grade.
  • Attitude in the laboratory: The laboratory grade, besides attendance, also considers the attitude towards the course (responsibility and behavior in the laboratory, punctuality, having read the practical in advance, use of the laboratory notebook, response to questions asked by the faculty in the laboratory, etc.). A minimum grade of 5 is required to pass the course.
  • Written exam: It will include questions on concepts, calculations, graph interpretation, etc., related to the practicals done in the laboratory. A minimum grade of 4 is required to average with the rest of the grades and pass the course.

The final grade for this part of the course will be calculated as: 15% laboratory attitude, 15% exam, and 70% reports.

Grades

A student will be considered Not Evaluated when one of the following situations occurs:

  • The percentage of completion of the Computer Science Fundamentals Practicals assessment activities is less than 67%.
  • The percentage of completion of the Chemical Engineering Laboratory Fundamentals Practicals assessment activities is less than 67%.
  • Attendance at laboratory practical sessions is less than 8 days, with or without justification.

The Honor Roll (MH) grade can be awarded starting from an average grade of 9.0 out of 10. The total number of MHs will never exceed 5% of the total enrolled students. To obtain the MH, a minimum grade of 8.5 in each course activity is required.

If the average grade of the two parts of the course (Computer Science or Laboratory) is 5 out of 10 or higher, but one of the parts has a grade below 5, the final grade for the course will correspond to the lowest grade.

Recovery Process

The recovery process is independent for each part of the course.

Computer Science Fundamentals Practicals

If the average grade of the exercises is less than 5.0 out of 10, this part of the course can be recovered in an exam that includes all the covered content and will replace the exercise grades. To participate in the recovery, the student must have been previously assessed in a set of activities whose weight equals at least two-thirds of the total grade for this part of the course.

The recovery exam will be conducted according to the schedule set by the coordination.

Chemical Engineering Fundamentals Laboratory Practicals

Only the exam is eligible for recovery, and a minimum grade of 4 on the recovery exam is required to pass the course. To be eligible for the recovery exam, the report grades must be equal to or higher than 5. If the exam grade is below 4, but the calculated overall grade is 5 or higher, the recorded grade for the laboratory partwill be the recovery exam grade.

The recovery exam will be conducted according to the schedule set by the coordination.

Grade Review Procedure

Students will have the opportunity to request a review of the various activities and reports submitted within 24 hours after the grade is published by contacting the instructor who graded the work to schedule a review, or by following the instructions provided for the reviews.

Student Irregularities, Cheating, and Plagiarism

Without prejudice to other disciplinary measures that may be deemed appropriate and in accordance with current academic regulations, any irregularities committed by the student that may lead to a variation in the evaluation grade will be graded with a zero.

Reports must be original. Copying a practice or part of a practice will result in a zero for that report. Copying is defined as the presence of identical paragraphs to other reports or a reinterpretation of them.It will also be considered copying if a report from another group is used as a model.

This course does not provide a single assessment system.


Bibliography

  • F. Charte Ojeda, Excel 2016. Anaya Multimedia 2016 ISBN: 9788441538061
  • M.B. Cutlip y M. Shacham. Resolución de problemas de Ingeniería Química y Bioquímica con Polymath, Excel y Matlab. Pearson Educación S.A. Madrid. 2008. ISBN: 978-84-8322-461-8.
  • Steven C. Chapra & Raymond P. Canale Métodos numéricos para ingenieros. Ed. (2003) McGrwHill. ISBN: 970-10-3965-3
  • CRC Handbook of Chemistry and Physics John R. Rumble, ed, 100th Edition CRC Press/Taylor & Francis, Boca Raton, FL.
  • Tosun "Modeling in Transport Phenomena. A Conceptual Approach", 2nd ed., Elsevier, 2007.
  • C.J. Geankoplis, “Transport Processes and Separation Process Principles”, 4th ed., Prentice Hall, 2003.
  • R.M. Felder, R.W. Rousseau, "Elementary Principles of Chemical Processes", 3rd ed., Wiley, 2000.
  • Perry's Chemical Engineers' Handbook, 7th ed., McGraw-Hill, 1997.
  • R.B. Bird, W.E. Stewart, E.N. Lightfoot "Transport Phenomena", 2nd ed. John Wiley & Sons, 2002.
  • R.C. Reid, J.M. Prausnitz, B.E. Poling "The Properties of Gases and Liquids", 4th ed. McGraw-Hill, 1987.
  • M.L. Sheely "Glycerol viscosity table" Industrial and Engineering Chemistry, 24(9), 1932, 1060-1064. 

Software

MS Word and MS Excel


Language list

Name Group Language Semester Turn
(PLAB) Practical laboratories 211 Catalan second semester morning-mixed
(PLAB) Practical laboratories 212 Catalan second semester morning-mixed
(PLAB) Practical laboratories 213 Catalan second semester morning-mixed
(PLAB) Practical laboratories 214 Catalan second semester morning-mixed
(TE) Theory 21 Catalan second semester morning-mixed